Spice Extraction-The FASA Approach - Revision history

TheTraveler at 19:34, 17 September 2013

2013-09-17T19:34:01Z

← Older revision		Revision as of 19:34, 17 September 2013
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	<references/>		<references/>

			[[Category:Conversion Tek]]
	[[Category:Method Tek]]		[[Category:Method Tek]]
	[[Category:DMT]]		[[Category:DMT]]

TheTraveler: Text replace - "dmt-nexus.com" to "dmt-nexus.me"

2012-01-31T19:56:56Z

Text replace - "dmt-nexus.com" to "dmt-nexus.me"

← Older revision		Revision as of 19:56, 31 January 2012
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	{{ShowInfo\|[[Image:Note_error.png]]\|'''Note:'''\|This page is a transcription of Spice Extraction-The FASA Approach by Infundibulum<ref>Spice Extraction-The FASA Approach by Infundibulum		{{ShowInfo\|[[Image:Note_error.png]]\|'''Note:'''\|This page is a transcription of Spice Extraction-The FASA Approach by Infundibulum<ref>Spice Extraction-The FASA Approach by Infundibulum
	[http://wiki.dmt-nexus.~~com~~/Image:SPICE_EXTRACTION-The_FASA_approach.pdf]</ref>. The content is to remain accurate as such.		[http://wiki.dmt-nexus.me/Image:SPICE_EXTRACTION-The_FASA_approach.pdf]</ref>. The content is to remain accurate as such.
	}}		}}

Endlessness: Undo revision 3505 by Alysia (Talk)

2010-07-10T03:17:20Z

Undo revision 3505 by Alysia (Talk)

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	[[Category:Method Tek]]		[[Category:Method Tek]]
	[[Category:DMT]]		[[Category:DMT]]
	~~[http://www.chatixdating.com/ Dating Chat]~~
	~~[http://www.teensay.com/ Teen Chat]~~

Alysia: /* Reference */

2010-07-10T02:46:00Z

Reference

← Older revision		Revision as of 02:46, 10 July 2010
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	[[Category:Method Tek]]		[[Category:Method Tek]]
	[[Category:DMT]]		[[Category:DMT]]
			[http://www.chatixdating.com/ Dating Chat]
			[http://www.teensay.com/ Teen Chat]

Endlessness: Undo revision 3498 by LoisTardy (Talk)

2010-07-04T05:52:26Z

Undo revision 3498 by LoisTardy (Talk)

← Older revision		Revision as of 05:52, 4 July 2010
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	== Reference ==		== Reference ==

	~~[http://www.superiorpapers.com/term_paper_writing_services.php writing services]~~

	<references/>		<references/>

	[[Category:Method Tek]]		[[Category:Method Tek]]
	[[Category:DMT]]		[[Category:DMT]]

LoisTardy: /* Reference */

2010-07-02T14:19:57Z

Reference

← Older revision		Revision as of 14:19, 2 July 2010
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	== Reference ==		== Reference ==

			[http://www.superiorpapers.com/term_paper_writing_services.php writing services]

	<references/>		<references/>

	[[Category:Method Tek]]		[[Category:Method Tek]]
	[[Category:DMT]]		[[Category:DMT]]

Geeg30: /* The TEK */

2009-04-16T00:41:33Z

The TEK

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	=== The TEK ===		=== The TEK ===
	Before one starts, FASA (fumaric acid saturated acetone) needs to be ~~generated~~. This is simply done by mixing an amount of fumaric acid and acetone and leaving it for a day or so to saturate completely. Acetone can hold ~20mg of fumaric acid per ml. ~~A guy that I vaguely know puts loads of~~ fumaric acid ~~in his~~ acetone ~~without weighting it. The~~ excess is just going to fall on the bottom and can be re-dissolved in fresh acetone if necessary.		Before one starts, FASA (fumaric acid saturated acetone) needs to be made. This is simply done by mixing an amount of fumaric acid and acetone and leaving it for a day or so to saturate completely. Acetone can hold ~20mg of fumaric acid per ml. It is not necessary to weigh the fumaric acid before mixing with the acetone as the excess is just going to fall on the bottom and can be re-dissolved in fresh acetone if necessary.

	As long as one has FASA handy, the next steps are:		As long as one has FASA handy, the next steps are:
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	{{ShowInfo/In Article\|[[Image:Information.png]]\|'''A REMARK'''\|		{{ShowInfo/In Article\|[[Image:Information.png]]\|'''A REMARK'''\|
	Theoretically any non-polar solvent can be used with the FASA tek. However, ~~this guy I vaguely know~~ observed that some brands of naphtha ~~caused~~ precipitation of the fumaric acid when FASA was added to them. If one wishes to use a non-polar solvent other than xylene/toluene he/she is strongly advised to test whether fumaric acid from FASA precipitates when added in clean, unused solvent.		Theoretically any non-polar solvent can be used with the FASA tek. However, it has been observed that some brands of naphtha cause the precipitation of the fumaric acid when FASA was added to them. If one wishes to use a non-polar solvent other than xylene/toluene he/she is strongly advised to test whether fumaric acid from FASA precipitates when added in clean, unused solvent.
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	=== Freebasing the fumarate salts ===		=== Freebasing the fumarate salts ===

TheTraveler: /* Introduction */

2009-04-15T20:59:48Z

Introduction

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	[[Image:Dmt fumarate bond.JPG\|thumb\|Two DMT molecules forming a complex with one fumaric acid molecule to form [[DMT Fumarate\|DMT Fumarate]].]]		[[Image:Dmt fumarate bond.JPG\|thumb\|Two DMT molecules forming a complex with one fumaric acid molecule to form [[DMT Fumarate\|DMT Fumarate]].]]
	=== Introduction ===		=== Introduction ===
	This document outlines recent advancement on the extraction of alkaloids from ~~DMTcontaining~~		This document outlines recent advancement on the extraction of alkaloids from DMT containing
	material making use of fumaric acid. This method is used in conjunction		material making use of fumaric acid. This method is used in conjunction
	with a standard [[:Category:Acid/Base\|A/B]] or [[:Category:Straight To Base\|STB]] tek and it has the following advantages:		with a standard [[:Category:Acid/Base\|A/B]] or [[:Category:Straight To Base\|STB]] tek and it has the following advantages:

TheTraveler at 20:58, 15 April 2009

2009-04-15T20:58:26Z

TheTraveler at 20:48, 15 April 2009

2009-04-15T20:48:11Z

← Older revision		Revision as of 20:48, 15 April 2009
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	=== The TEK ===		=== The TEK ===
	Before one starts, FASA (fumaric acid saturated acetone) needs to be generated. This is simply done by mixing an amount of fumaric acid and acetone and leaving it for a day or so to saturate completely. Acetone can hold ~20mg of fumaric acid per ml. A guy that I vaguely know puts loads of fumaric acid in his acetone without weighting it. The excess is just going to fall on the bottom and can be dissolved ~~from~~ fresh acetone if necessary.		Before one starts, FASA (fumaric acid saturated acetone) needs to be generated. This is simply done by mixing an amount of fumaric acid and acetone and leaving it for a day or so to saturate completely. Acetone can hold ~20mg of fumaric acid per ml. A guy that I vaguely know puts loads of fumaric acid in his acetone without weighting it. The excess is just going to fall on the bottom and can be re-dissolved in fresh acetone if necessary.

	As long as one has FASA handy, the next steps are:		As long as one has FASA handy, the next steps are:
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	{{ShowInfo/In Article\|[[Image:Information.png]]\|'''WHAT IS HAPPENING INSIDE THE NON-POLAR SOLVENT?'''\|		{{ShowInfo/In Article\|[[Image:Information.png]]\|'''WHAT IS HAPPENING INSIDE THE NON-POLAR SOLVENT?'''\|
	The xylene/toluene pull contains the freebased DMT, the freebased DMT-~~NOxide~~ (in the case of old material where part of DMT has oxidised), Jungle Spice (in the case of MHRB) as well as any other lipid impurities that are picked up by the solvent.		The xylene/toluene pull contains the freebased DMT, the freebased DMT-''n''-oxide (in the case of old material where part of DMT has oxidised), Jungle Spice (in the case of MHRB) as well as any other lipid impurities that are picked up by the solvent.

	Addition of FASA introduces fumaric acid in the xylene/toluene and this reacts immediately with the freebased DMT, the freebased DMT N-~~Oxide~~ and Jungle spice to form their respective fumarate salts. DMT-fumarate, DMT-N-~~Oxide~~-fumarate and Jungle spice-fumarate precipitate out since they are insoluble in xylene/toluene as well as acetone.		Addition of FASA introduces fumaric acid in the xylene/toluene and this reacts immediately with the freebased DMT, the freebased DMT-''n''-oxide and Jungle spice to form their respective fumarate salts. DMT-fumarate, DMT-''n''-oxide-fumarate and Jungle spice-fumarate precipitate out since they are insoluble in xylene/toluene as well as acetone.

	In contrast, any lipid impurities and any not interesting compounds will be left behind.		In contrast, any lipid impurities and any not interesting compounds will be left behind.
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	{{ShowInfo/In Article\|[[Image:Information.png]]\|'''NOTE'''\|		{{ShowInfo/In Article\|[[Image:Information.png]]\|'''NOTE'''\|
	The fumarate salts of DMT, DMT-N-~~Oxide~~ and Jungle Spice tend to be a bit hygroscopic, that is they have a gooey consistency upon drying. Given time however, they dry to rock-hard consistency. One is fine drying the salts in the oven at 50 Celsius, this makes things much faster.		The fumarate salts of DMT, DMT-''n''-oxide and Jungle Spice tend to be a bit hygroscopic, that is they have a gooey consistency upon drying. Given time however, they dry to rock-hard consistency. One is fine drying the salts in the oven at 50 Celsius, this makes things much faster.
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	That’s it! One now has the plant’s alkaloids in fumarate salt. They can be eaten,		That’s it! One now has the plant’s alkaloids in fumarate salt. They can be eaten,
	snorted or freebased for smoking. Note that the use of xylene/toluene pulls more		snorted or freebased for smoking. Note that the use of xylene/toluene pulls more
	things out of the plants, such as DMT-N-~~Oxide~~ which is insoluble to naphtha. The		things out of the plants, such as DMT-''n''-oxide which is insoluble to naphtha. The
	next session describes how the fumarate salts can be freebased.		next session describes how the fumarate salts can be freebased.

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	{{In_Article/ABC_Line\|F)\|Step D can be repeated 4-5 times just to make sure all the freebase had been picked up.}}		{{In_Article/ABC_Line\|F)\|Step D can be repeated 4-5 times just to make sure all the freebase had been picked up.}}

	{{In_Article/ABC_Line\|G)\|The freebase that results is a mixture of all the different alkaloids that can be pulled using xylene/toluene. This may take some time to get solid, especially if plenty of DMT-N-~~Oxide~~ is present. DMT-N-~~Oxide~~ is a yellow oil and albeit perfectly smokable and pretty active it can hinder the solidification of the end product. But given time, it does get solid. And it provides a very intense experience. Alternatively……}}		{{In_Article/ABC_Line\|G)\|The freebase that results is a mixture of all the different alkaloids that can be pulled using xylene/toluene. This may take some time to get solid, especially if plenty of DMT-''n''-oxide is present. DMT-''n''-oxide is a yellow oil and albeit perfectly smokable and pretty active it can hinder the solidification of the end product. But given time, it does get solid. And it provides a very intense experience. Alternatively……}}

	{{In_Article/ABC_Line\|H)\|(Optional)…..one may wish to get pure white DMT out of this mixture. In that case the freebased alkaloids can be washed with naphtha. Naphtha will pick all DMT leaving back DMT-N-~~Oxide~~ and [[Jungle Spice]] (if [[MHRB]] had been used).}}		{{In_Article/ABC_Line\|H)\|(Optional)…..one may wish to get pure white DMT out of this mixture. In that case the freebased alkaloids can be washed with naphtha. Naphtha will pick all DMT leaving back DMT-''n''-oxide and [[Jungle Spice]] (if [[MHRB]] had been used).}}

	== Reference ==		== Reference ==

← Older revision		Revision as of 20:58, 15 April 2009
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	This document outlines recent advancement on the extraction of alkaloids from DMTcontaining		This document outlines recent advancement on the extraction of alkaloids from DMTcontaining
	material making use of fumaric acid. This method is used in conjunction		material making use of fumaric acid. This method is used in conjunction
	with a standard A/B or STB tek and it has the following advantages:		with a standard [[:Category:Acid/Base\|A/B]] or [[:Category:Straight To Base\|STB]] tek and it has the following advantages:
	# ''It requires no defatting of the plant material''. Even leafy material that is notoriously high in oils requires NO defatting. Pure white DMT has been extracted from Diplopterys cabrerana using FASA with the same easiness and defat-free steps as with MHRB.		# ''It requires no defatting of the plant material''. Even leafy material that is notoriously high in oils requires NO defatting. Pure white DMT has been extracted from [[Diplopterys cabrerana]] using [[FASA]] with the same easiness and defat-free steps as with [[MHRB]].
	# ''It requires no recrystallisation of the product'' neither any freeze precipitations. One may however try to crystallise the final product if one wants to create big crystals		# ''It requires no recrystallisation of the product'' neither any freeze precipitations. One may however try to crystallise the final product if one wants to create big crystals
	# ''One knows exactly when to stop pulling'' when using the non-polar solvent		# ''One knows exactly when to stop pulling'' when using the non-polar solvent
	# ''The NP solvent can be used again and again and again''. That is, there is no need for evaporation of the NP solvent. This saves money, it is minimally smelly and more eco-friendly.		# ''The NP solvent can be used again and again and again''. That is, there is no need for evaporation of the NP solvent. This saves money, it is minimally smelly and more eco-friendly.
	# ''The initial product of this extraction is a stable dmt salt (~~dmt fumarate~~)'' that can be used as such (snorted or orally in conjunction with a MAOI), stored for long periods of time or freebased for smoking.		# ''The initial product of this extraction is a stable dmt salt ([[DMT Fumarate]])'' that can be used as such ([[Insuffulation\|snorted]] or orally in conjunction with a [[MAOI]]), stored for long periods of time or freebased for smoking.

	=== The Theory ===		=== The Theory ===
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	{{ShowInfo/In Article\|[[Image:Information.png]]\|'''WHAT IS HAPPENING INSIDE THE NON-POLAR SOLVENT?'''\|		{{ShowInfo/In Article\|[[Image:Information.png]]\|'''WHAT IS HAPPENING INSIDE THE NON-POLAR SOLVENT?'''\|
	The xylene/toluene pull contains the freebased DMT, the freebased DMT-''n''-oxide (in the case of old material where part of DMT has oxidised), Jungle Spice (in the case of MHRB) as well as any other lipid impurities that are picked up by the solvent.		The xylene/toluene pull contains the freebased DMT, the freebased [[DMT-n-oxide\|DMT-''n''-oxide]] (in the case of old material where part of DMT has oxidised), [[Jungle Spice]] (in the case of [[MHRB]]) as well as any other lipid impurities that are picked up by the solvent.

	Addition of FASA introduces fumaric acid in the xylene/toluene and this reacts immediately with the freebased DMT, the freebased DMT-''n''-oxide and Jungle ~~spice~~ to form their respective fumarate salts. DMT-fumarate, DMT-''n''-oxide-fumarate and Jungle spice-fumarate precipitate out since they are insoluble in xylene/toluene as well as acetone.		Addition of FASA introduces fumaric acid in the xylene/toluene and this reacts immediately with the freebased DMT, the freebased [[DMT-n-oxide\|DMT-''n''-oxide]] and [[Jungle Spice]] to form their respective fumarate salts. DMT-fumarate, DMT-''n''-oxide-fumarate and Jungle spice-fumarate precipitate out since they are insoluble in xylene/toluene as well as acetone.

	In contrast, any lipid impurities and any not interesting compounds will be left behind.		In contrast, any lipid impurities and any not interesting compounds will be left behind.