Limtek Extraction - Revision history

TheTraveler: Text replace - "dmt-nexus.com" to "dmt-nexus.me"

2012-01-31T19:56:30Z

Text replace - "dmt-nexus.com" to "dmt-nexus.me"

← Older revision		Revision as of 19:56, 31 January 2012
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	: [[:Category:Limtek\|Directory of Current Limteks]]		: [[:Category:Limtek\|Directory of Current Limteks]]
	: [http://dmt-nexus.~~com~~/forum/default.aspx?g=posts&t=8503 A Poll to Gauge Members' Success w/ Lime]		: [http://dmt-nexus.me/forum/default.aspx?g=posts&t=8503 A Poll to Gauge Members' Success w/ Lime]
	: [http://dmt-nexus.~~com~~/forum/default.aspx?g=posts&t=7829 Pickling lime instead of lye?]		: [http://dmt-nexus.me/forum/default.aspx?g=posts&t=7829 Pickling lime instead of lye?]
	: [http://dmt-nexus.~~com~~/forum/default.aspx?g=posts&t=7743 Calcium Hydroxide instead of lye?]		: [http://dmt-nexus.me/forum/default.aspx?g=posts&t=7743 Calcium Hydroxide instead of lye?]

	<noinclude>{{Page_Footer\|Limtek}}</noinclude>		<noinclude>{{Page_Footer\|Limtek}}</noinclude>

Amor fati: footer/categorization

2011-02-08T16:12:17Z

footer/categorization

← Older revision		Revision as of 16:12, 8 February 2011
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	: [http://dmt-nexus.com/forum/default.aspx?g=posts&t=7829 Pickling lime instead of lye?]		: [http://dmt-nexus.com/forum/default.aspx?g=posts&t=7829 Pickling lime instead of lye?]
	: [http://dmt-nexus.com/forum/default.aspx?g=posts&t=7743 Calcium Hydroxide instead of lye?]		: [http://dmt-nexus.com/forum/default.aspx?g=posts&t=7743 Calcium Hydroxide instead of lye?]

			<noinclude>{{Page_Footer\|Limtek}}</noinclude>

Amor fati: /* Extraction Procedure */

2010-01-24T20:16:24Z

Extraction Procedure

← Older revision		Revision as of 20:16, 24 January 2010
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	#* ''this is the most important part for a successful yield, and due to the lack of a proper aqueous phase, the reaction requires a stronger degree of manual facilitation.''		#* ''this is the most important part for a successful yield, and due to the lack of a proper aqueous phase, the reaction requires a stronger degree of manual facilitation.''
	# Wash the mixture with [[NPS]] by stirring and decanting to collect the [[NPS]], and proceed to the appropriate desired [[The_Nexian_DMT_Handbook#Crystallization\|crystallization]] method.		# Wash the mixture with [[NPS]] by stirring and decanting to collect the [[NPS]], and proceed to the appropriate desired [[The_Nexian_DMT_Handbook#Crystallization\|crystallization]] method.
	#* ''the more contact brought between the material and the target solvent, the more successful the ~~reaction~~ will be.''		#* ''the more contact brought between the material and the target solvent, the more successful the extraction will be.''

	====='''Further Elaboration and Technical Support'''=====		====='''Further Elaboration and Technical Support'''=====

Amor fati: /* Extraction Procedure */

2010-01-13T15:25:14Z

Extraction Procedure

← Older revision		Revision as of 15:25, 13 January 2010
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	# Thoroughly moisten the mixture while stirring, ensuring that no dry spots remain and the mixture exhibits a doughy or pasty consistency.		# Thoroughly moisten the mixture while stirring, ensuring that no dry spots remain and the mixture exhibits a doughy or pasty consistency.
	#* ''the added water facilitates reaction and a basic environment which may aid in breaking down the plant material.''		#* ''the added water facilitates reaction and a basic environment which may aid in breaking down the plant material.''
	#* ''the acid component of the natural salt-form of the product within the plant material will neutralized, yielding a freebase product.''		#* ''the acid component of the natural salt-form of the product within the plant material will be neutralized, yielding a freebase product.''
	# Ensure a thoroughly homogeneous mixture and allot enough time and stirring for a complete reaction.		# Ensure a thoroughly homogeneous mixture and allot enough time and stirring for a complete reaction.
	#* ''this is the most important part for a successful yield, and due to the lack of a proper aqueous phase, the reaction requires a stronger degree of manual facilitation.''		#* ''this is the most important part for a successful yield, and due to the lack of a proper aqueous phase, the reaction requires a stronger degree of manual facilitation.''

Amor fati: /* Overview of Materials and Methods */

2010-01-13T15:04:25Z

Overview of Materials and Methods

← Older revision		Revision as of 15:04, 13 January 2010
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	* Water		* Water
	* [[NPS]]		* [[NPS]]
	** Typically d-Limonene		** Typically [[d-Limonene]]
	\|		\|
	* Calcium Hydroxide (Pickling Lime)		* [[Calcium Hydroxide]] (Pickling Lime)
	}}		}}

	Material Considerations:		Material Considerations:
	* In order for the process to remain nontoxic, an aqueous food-grade acid should be used to salt out of the product.		* In order for the process to remain nontoxic, an aqueous food-grade acid should be used to salt out of the product.
	** ''FASW (Fumaric Acid Saturated Water) can be evaporated to achieve a crystalline DMT fumarate.''		** ''[[FASW]] (Fumaric Acid Saturated Water) can be evaporated to achieve a crystalline [[DMT fumarate]].''
	** ''vinegar can be used to achieve DMT acetate but will not crystallize.''		** ''vinegar can be used to achieve [[DMT acetate]] but will not crystallize.''
	* Limonene can be replaced with other [[NPS]]'s, but the process will cease to be nontoxic.		* Limonene can be replaced with other [[NPS]]'s, but the process will cease to be nontoxic.

Amor fati at 15:02, 13 January 2010

2010-01-13T15:02:49Z

← Older revision		Revision as of 15:02, 13 January 2010
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	** Typically d-Limonene		** Typically d-Limonene
	\|		\|
	* Household Base:		* Calcium Hydroxide (Pickling Lime)
	** Calcium Hydroxide (Pickling Lime)
	}}		}}

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	Methods:		Methods:
	: Extraction by limtek is characterized by the lack of a proper aqueous phase but also the lack of necessity for drying procedures, and essentially involves a pasty or ~~dough~~ material being washed in the target solvent to retrieve product.		: Extraction by limtek is characterized by the lack of a proper aqueous phase but also the lack of necessity for drying procedures, and essentially involves a pasty or doughy material being washed in the target solvent to retrieve product.

	====Extraction Procedure====		====Extraction Procedure====

Amor fati: /* Extraction Procedure */

2010-01-01T20:14:19Z

Extraction Procedure

← Older revision		Revision as of 20:14, 1 January 2010
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	#* ''this is the most important part for a successful yield, and due to the lack of a proper aqueous phase, the reaction requires a stronger degree of manual facilitation.''		#* ''this is the most important part for a successful yield, and due to the lack of a proper aqueous phase, the reaction requires a stronger degree of manual facilitation.''
	# Wash the mixture with [[NPS]] by stirring and decanting to collect the [[NPS]], and proceed to the appropriate desired [[The_Nexian_DMT_Handbook#Crystallization\|crystallization]] method.		# Wash the mixture with [[NPS]] by stirring and decanting to collect the [[NPS]], and proceed to the appropriate desired [[The_Nexian_DMT_Handbook#Crystallization\|crystallization]] method.
	#* ''the more contact brought between the material and the solvent, the more successful the reaction will be.''		#* ''the more contact brought between the material and the target solvent, the more successful the reaction will be.''

	====='''Further Elaboration and Technical Support'''=====		====='''Further Elaboration and Technical Support'''=====

Amor fati: /* Extraction Procedure */

2010-01-01T20:13:52Z

Extraction Procedure

← Older revision		Revision as of 20:13, 1 January 2010
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	# Ensure a thoroughly homogeneous mixture and allot enough time and stirring for a complete reaction.		# Ensure a thoroughly homogeneous mixture and allot enough time and stirring for a complete reaction.
	#* ''this is the most important part for a successful yield, and due to the lack of a proper aqueous phase, the reaction requires a stronger degree of manual facilitation.''		#* ''this is the most important part for a successful yield, and due to the lack of a proper aqueous phase, the reaction requires a stronger degree of manual facilitation.''
	# Wash the mixture with ~~limonene~~ by stirring and decanting to collect the ~~limonene~~, and proceed to the appropriate desired [[The_Nexian_DMT_Handbook#Crystallization\|crystallization]] method.		# Wash the mixture with [[NPS]] by stirring and decanting to collect the [[NPS]], and proceed to the appropriate desired [[The_Nexian_DMT_Handbook#Crystallization\|crystallization]] method.
	#* ''the more contact brought between the material and the solvent, the more successful the reaction will be.''		#* ''the more contact brought between the material and the solvent, the more successful the reaction will be.''

Amor fati: /* Overview of Materials and Methods */

2010-01-01T20:10:55Z

Overview of Materials and Methods

← Older revision		Revision as of 20:10, 1 January 2010
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	\|		\|
	* Water		* Water
	* d-Limonene		* [[NPS]]
			** Typically d-Limonene
	\|		\|
	* Household Base:		* Household Base:

Amor fati: /* Further Elaboration and Technical Support */

2010-01-01T19:57:48Z

Further Elaboration and Technical Support

← Older revision		Revision as of 19:57, 1 January 2010
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	====='''Further Elaboration and Technical Support'''=====		====='''Further Elaboration and Technical Support'''=====

	: [[:Category:Limtek\|~~List~~ of Current Limteks]]		: [[:Category:Limtek\|Directory of Current Limteks]]
	: [http://dmt-nexus.com/forum/default.aspx?g=posts&t=8503 A Poll to Gauge Members' Success w/ Lime]		: [http://dmt-nexus.com/forum/default.aspx?g=posts&t=8503 A Poll to Gauge Members' Success w/ Lime]
	: [http://dmt-nexus.com/forum/default.aspx?g=posts&t=7829 Pickling lime instead of lye?]		: [http://dmt-nexus.com/forum/default.aspx?g=posts&t=7829 Pickling lime instead of lye?]
	: [http://dmt-nexus.com/forum/default.aspx?g=posts&t=7743 Calcium Hydroxide instead of lye?]		: [http://dmt-nexus.com/forum/default.aspx?g=posts&t=7743 Calcium Hydroxide instead of lye?]